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Thermal ionization mass spectrometry (TIMS): silicate digestion, separation, and measurement

By: Makishima, AkioMaterial type: TextTextLanguage: English Publication details: Weinheim: Wiley-VCH, 2016 Description: xxi,347p. PbkISBN: 9783527340248Subject(s): MASS SPECTROMETRY | ANALYTICAL GEOCHEMISTRY | GEOCHEMISTRYDDC classification: 550.4 Summary: This first book to discuss both separation chemistry and mass spectrometry for mineral and rock analysis compares the two frequently used techniques, analyzing both their scope and limitations by way of numerous practical examples. The excellent and highly experienced author adopts a comprehensive and systematic approach, reviewing all the steps involved in an analytical workflow. In addition to thermal ionization mass spectrometry (TIMS), he also discusses applications of ICP-MS. Furthermore, alongside detailed protocols on sample preparation and mass spectrometric measurements, numerous practical hints are given. A must-have handy guide for all isotope geochemists and anyone involved in isotope analysis.
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Table of Contents

Preface IX
1 Analytical Geochemistry
2 Basics and Principles of Sample Digestion
3 Basics and Principles of Chemical Separation
4 Mass Spectrometry
5 Techniques in TIMS
6 Application of TIMS to Isotopic Ratio Analysis of Each Element
7 Conclusions
Appendix A: Bulk Analysis and Spot Analysis
Appendix B: Laser Ablation-Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS)
References
Index

This first book to discuss both separation chemistry and mass spectrometry for mineral and rock analysis compares the two frequently used techniques, analyzing both their scope and limitations by way of numerous practical examples.
The excellent and highly experienced author adopts a comprehensive and systematic approach, reviewing all the steps involved in an analytical workflow. In addition to thermal ionization mass spectrometry (TIMS), he also discusses applications of ICP-MS. Furthermore, alongside detailed protocols on sample preparation and mass spectrometric measurements, numerous practical hints are given.
A must-have handy guide for all isotope geochemists and anyone involved in isotope analysis.

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